Parameter Set
|
SELNOGP |
Pulse Sequence |
selnogp |
| Experiment Description |
-
- Selective NOESY is a 1D experiment which determines the NOE correlation of one specific site.
- One peak is selected and signal is transferred from it to all protons in the vicinity of its location that are dipolar coupled to it.
|
Scans
(ns) |
Dummy Scans
(ds) |
Recycle
Delay
(d1) |
1D
Loop
(TD0) |
FID Size
(TD, F2) |
Spectral
Width
(sw,ppm) |
Spectral
Center
(o1p, ppm) |
| 2 x ns (32) |
4 |
2 |
1 |
64k |
20 |
6.18 |
| Experiment Setup |
-
- Use getprosol or prosol button to read in proper pulse parameters
- d8 is the mixing time (default 300 ms); must be long enough for NOE build up.
- Small molecules: d8 = T1
- Large molecules: d8 = 0.5 T1
- spoffs1 is the offset frequency of the shaped pulse.
- Find the center frequency of the spectrum (sw)
- Find the frequency of the site you want to irradiate with the shaped pulse (use cursor)
|
| Processing Notes |
|
| Sample Spectrum |
|
